1402029N enthalpy .pdf


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Testing Cert. # 3198.01

Company
Analyst
Parameters
Job #

NicVape Inc.
KEH
GC Analysis
0314-27

# Samples 1
Sample(s) Received 03/04/2014

Enthalpy Code

Client's Sample ID

0314-27-07

1402029N-100PG

Batch/Lot/Notes

Nicotine
(mg/mL)
99.4

Summary of Method:
A measured volume of each sample is transferred to a 15-mL conical tube. The samples
are then diluted with 2-propanol and a known amount of n-heptadecane is added to each
sample. N-heptadecane serves as an internal standard and improves the accuracy and
precision of the method. N-heptadecane is not present in native e-liquids. An aliquot of
the diluted sample is then removed for analysis by gas chromatography with flame
ionization detection (GC-FID). Samples are quantitated against a calibration curve
containing known amounts of nicotine and n-heptadecane. Note that other peaks may be
seen in the chromatograms including propylene glycol, glycerin, and various flavor
compounds, if present.

I certify that to the best of my knowledge all analytical data presented in this report:
• Have been checked for completeness
• Are accurate, error-free, and legible
• Have been conducted in accordance with approved protocol, and that all deviations
and analytical problems are summarized.
This analytical report was prepared in Portable Document Format (.PDF) and contains 2 pages.

Report Issued: 03/13/2014

Enthalpy Analytical, Inc.
Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com
800-1 Capitola Drive Durham, NC 27713-4385

Sample Report

Data file:
Sample name:
Description:

C:\CHEM32\1\DATA\R030514A\019B2101.D
0314-27-07

Instrument:

Ricky

Injection date:

3/5/2014 10:04:37 PM

Acq. method:
Analysis method:
Last changed:

R030514.M
3/10/2014 11:49:47 AM

Sequence_Name

Sample_Multipliers

1

Location:
Injection:

R030514A
Vial 19
1 of 1

Injection_Volume
Acq. operator:

1
Kathy Humphries

Sample_DilutionFactors

200

N-heptadecane added during analysis, used for quantitation only

Signal:

FID2 B,

RT [min] Type
7.063 BB

Area Amount Name
(mg/ml)
292923.81

99.38 Nicotine

E-liquid Template with internal note [Rev. 19]

per ml of liquid

Printed: 03/10/2014 11:58:17


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